Setting time evaluation of injectable carbonate apatite cement using various sodium carboxymethylcellulose (Na CMC) concentration

Padjadjaran Journal of Dentistry

Arief Cahyanto¹  Renny Febrida¹  Indah Permatasari¹ 

[1] Universitas Padjadjaran

关键词: Injectable carbonate apatite cement;    setting time;    sodium carboxymethylcellulose.;   

DOI  :  10.24198/pjd.vol30no2.18321

学科分类：口腔科学

来源: Universitas Padjadjaran

【 摘 要 】

Introduction:The injectable calcium phosphate cement has the advantage to be used in the bone defect with the limited access which supports a minimally invasive surgical technique. These Injectability properties of calcium phosphate cement can be modified by adding a sodium carboxymethylcellulose (Na CMC). The aim of this present study is to investigate the setting time of injectable bone cement based on CO 3 Ap using various Na CMC concentration.Methods:Vaterite (a polymorph of CaCO 3 ) and Dicalcium Phosphate Anhydrous (DCPA) as powder phase mixed with 0.2 mol/L Na 2 HPO 4solution containing 1% polyethylene glycol (PEG) and various concentration of Na CMC as followed 0.5%, 1%, 1.5%, and 2%, respectively. Each concentration groups was consisting of 5 samples from total 20 samples. Powder and liquid phase was mixed with a spatula at a liquid to powder (L/P) ratio of 0.4. The setting time of CO 3 Ap cement was evaluated according to the modification method standardized by ISO 1566 for dental zinc phosphate cement using a custom fabricated Vicat needle apparatus. The cement was maintained at 37ºC and 100% relative humidity as a standard requirement.Results:The mean value of setting time cement was as followed 0.5% Na CMC 35:06 minutes, 1% Na CMC 38:48 minutes, 1.5% Na CMC 40:06 minutes, and 2% Na CMC 41:30 minutes. The result is statistically significant ( p <0.05) with the group of 0.5% Na CMC compared to others group.Conclusion : Increasing the concentration of Na CMC could prolong the setting time of CO 3 Ap cement.

【 授权许可】

CC BY