New practical method of homogeneous dispersion of multi-walled carbon nanotubes (MWCNTs) into Mg matrix composites

17th IUMRS International Conference in Asia

Zhang, Teng^1 ; Du, Shuangming^1 ; Sun, Wanchang^1 ; Zhang, Jumei^1 ; Niu, Libin^1 ; Hua, Xiaohu^1

School of Material Science and Engineering, Xi'An University of Science and Technology, Xi'an

710054, China^1

关键词: Directional arrangements;    Dispersion methods;    Field emission scanning electron microscopy;    High-specific surfaces;    Homogeneous dispersions;    Magnesium matrix composite;    Magnesium substrates;    Mg matrix composites;   

Others  :  https://iopscience.iop.org/article/10.1088/1757-899X/182/1/012028/pdf
DOI  :  10.1088/1757-899X/182/1/012028

来源: IOP

【 摘 要 】

It is difficult to disperse multi-walled carbon nanotubes (MWCNTs) into Mg matrix composites homogeneously due to the high specific surface energy between MWCNTs. This would affect the mechanical properties of magnesium matrix composites reinforced by MWCNTs tremendously. The key is to overcome MWCNTs aggregate together, and gain the homogeneous dispersion of MWCNTs. Moreover, the density difference of Mg matrix and MWCNTs is another problem which prevents MWCNTs from dispersing homogeneously into Mg matrix composites. In order to solve these problems, a new practical method of homogeneous dispersion of carbon nanotubes into Mg matrix composites was presented basing on combination the tow step ball milling and ultrasonication dispersion methods. First, a certain amount of MWCNTs was ball-milled in ethanol solution contain 5 wt.% sodium stearate at various rotation speeds (100 rpm-300 rpm) and ball-milled times (0.5 H-2 H) to break MWCNTs hard aggregation. Second, MWCNTs which were subjected to the ball-milling were dispersed further in ethanol solution containing (SDS, DBS) using ultrasonication method. Third, the Mg powers were mixed with good dispersion of carbon nanotubes solution and ball-milled for 1 H to make MWCNTs coated uniformly on the surface of the magnesium substrate. The results were mainly examined by field emission scanning electron microscopy (SEM). It was found that MWCNTs were dispersed well and some of these MWCNTs had directional arrangement. Furthermore, MWCNTs were homogeneously dispersed into Mg matrix composites. These results suggest that this method has good application for magnesium matrix composites reinforced by carbon nanotubes.