Yttria-Stabilized Zirconia Ceramic Deposition on SS430 Ferritic Steel Grown by PLD - Pulsed Laser Deposition Method

International Conference on Advances in Nuclear Science and Engineering 2015

Rivai, Abu Khalid^1 ; Mardiyanto^1 ; Agusutrisno^2 ; Suharyadi, Edi^2

Center For Science and Technology of Advanced Materials - National Nuclear Energy Agency of Indonesia BATAN, Kawasan PUSPIPTEK Gd. 71, Tangerang Selatan

Banten

15314, Indonesia^1

Dept. of Physics, Faculty of Mathematics and Natural Science, Gadjah Mada University, Bulaksumur

Daerah Istimewa Yogyakarta

55281, Indonesia^2

关键词: Advanced nuclear reactors;    Energy dispersive x-ray;    High temperature materials;    Science and Technology;    Substrate temperature;    Thermal barrier coating (TBC);    X ray diffractometers;    Ytrria-stabilized zirconias;   

Others  :  https://iopscience.iop.org/article/10.1088/1742-6596/799/1/012016/pdf
DOI  :  10.1088/1742-6596/799/1/012016

来源: IOP

【 摘 要 】

Development of high temperature materials are one of the key issues for the deployment of advanced nuclear reactors due to higher temperature operation. One of the candidate materials for that purpose is ceramic-coated ferritic steel that one of the functions is to be a thermal barrier coating (TBC). Thin films of YSZ (Ytrria-Stabilized Zirconia) ceramic have been deposited on a SS430 ferritic steel using Pulsed Laser Deposition (PLD) at Center For Science and Technology of Advanced Materials laboratory - National Nuclear Energy Agency of Indonesia (BATAN). The thin film was deposited with the chamber pressure range of 200-225 mTorr, the substrate temperature of 800°C, and the number of laser shots of 3×104, 6×104and 9×104. Afterward, the samples were analyzed using Scanning Electron Microscope - Energy Dispersive X-ray Spectroscope (SEM-EDS), X-Ray Diffractometer (XRD), Atomic Force Microscope (AFM) and Vickers hardness tester. The results showed that the YSZ could homogeneously and sticky deposited on the surface of the ferritic steel. The surfaces were very smoothly formed with the surface roughness was in the range of 70 nm. Furthermore, thickness, composition of Zr4+dan Y3+, the crystallinity, and hardness property was increased with the increasing the number of the shots.