Co (II) Complexes with Schiff Base Ligands: Synthesis and EXAFS Study

International Conference on Recent Trends in Physics 2016

Mishra, Ashutosh^1 ; Mansuri, Amantulla^1 ; Ninama, Samrath^2 ; Trivedi, Apurva^3 ; Patidar, Sushma^1 ; Jamod, Mahesh^1 ; Awate, Ruchita^1

School of Physics, Devi Ahilya University, Khandwa Road Campus, Indore

452001, India^1

Kasturbagram Rural Institute, Kasturbagram Indore

452001, India^2

SICA College, Indore

452003, India^3

关键词: Beam lines;    Conventional methods;    EXAFS studies;    O- phenylenediamine;    Salicylaldehyde;    Schiff base complexes;    Schiff-base ligands;    Synchrotron radiation source;   

Others  :  https://iopscience.iop.org/article/10.1088/1742-6596/755/1/012031/pdf
DOI  :  10.1088/1742-6596/755/1/012031

来源: IOP

【 摘 要 】

Thesynthesis of transition metal Schiff base complexes of Co(II) are prepared by chemical root method. Obtained by the condensation of O-phenylenediamine, salicylaldehyde and isatin / 2-hydroxy- 1 Naphthaldehyde is presented. The complexes were characterized by Co- K- edge EXAFS measurements using the dispersive beam line at 2.5GeV energy of Indus-2 synchrotron radiation source RRCAT Indore. The recorded EXAFS data were analyzed using the computer software Athena for determine the nearest neighboring distances (bond lengths) of these complexes with conventional methods and were compared with Fourier transform (FT) analysis.