The effects of fuel type in synthesis of NiFe2O4 nanoparticles by microwave assisted combustion method

International Physics Conference at the Anatolian Peak 2016

Karaka, Zeynep Karciolu^1 ; Boncukçuolu, Recep^1 ; Karaka, Ibrahim H.^2

Environmental Engineering Department, Atatürk University, Erzurum

25240, Turkey^1

Chemical Engineering Department, Bayburt University, Erzurum

69000, Turkey^2

关键词: Brunauer Emmet Teller surface area;    Fully compatible;    Magnetic properties of nanoparticle;    Microwave-assisted combustions;    Nanoparticle synthesis;    Powder diffraction;    Reflection peaks;    Vibrating sample magnetometry;   

Others  :  https://iopscience.iop.org/article/10.1088/1742-6596/707/1/012046/pdf
DOI  :  10.1088/1742-6596/707/1/012046

来源: IOP

【 摘 要 】

In this study, it was investigated the effects of the used fuels on structural, morphological and magnetic properties of nanoparticles in nanoparticle synthesis with microwave assisted combustion method with an important method in quick, simple and low cost at synthesis of the nanoparticles. In this aim, glycine, urea and citric acid were used as fuel, respectively. The synthesised nanoparticles were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Brunauer-Emmet-Teller surface area (BET), and vibrating sample magnetometry (VSM) techniques. We observed that fuel type is quite effective on magnetic properties and surface properties of the nanoparticles. X-ray difractograms of the obtained nanoparticles were compared with standard powder diffraction cards of NiFe2O4(JCPDS Card Number 54-0964). The results demonstrated that difractograms are fully compatible with standard reflection peaks. According to the results of the XRD analysis, the highest crystallinity was observed at nanoparticles synthesized with glycine. The results demonstrated that the nanoparticles prepared with urea has the highest surface area. The micrographs of SEM showed that all of the nanoparticles have nano-crystalline behaviour and particles indication cubic shape. VSM analysis demonstrated that the type of fuel used for synthesis is highly effective a parameter on magnetic properties of nanoparticles.