Synthesis of Ti3SiC2-based composites by spark plasma sintering of preceramic papers

16th International Conference of Students and Young Scientists "Prospects of Fundamental Sciences Development"

自然科学（总论）

Kashkarov, E.B.^1 ; Syrtanov, M.S.^1 ; Sedanova, E.P.^1 ; Ivashutenko, A.S.^1 ; Lider, A.M.^1 ; Travitzky, N.^1^2

National Research Tomsk Polytechnic University, Tomsk

634050, Russia^1

Friedrich-Alexander-Universitt Erlangen-Nürnberg, Erlangen

91054, Germany^2

关键词: Effect of temperature;    Elemental compositions;    Energy dispersive X ray spectroscopy;    Phase and microstructures;    Sintered materials;    Sintering process;    Spark plasma sintering method;    Synthesis temperatures;   

Others  :  https://iopscience.iop.org/article/10.1088/1757-899X/597/1/012058/pdf
DOI  :  10.1088/1757-899X/597/1/012058

学科分类：自然科学（综合）

来源: IOP

【 摘 要 】

This paper is devoted to fabrication of Ti3SiC2-based ceramic materials from preceramic paper using spark plasma sintering (SPS) method. The synthesis temperature and pressure were 1373-1473 K and 30 MPa, respectively. The phase composition, microstructure and elemental composition were analysed using X-ray diffraction, scanning electron microscopy and energy-dispersive X-ray spectroscopy, respectively. The effect of temperature on the sintering process as well as on the phase and microstructure of the sintered materials was investigated.