Application of Box_Behnken design with Response Surface Methodology for Modeling and Optimizing Microwave-assisted Hydro-distillation of Essential Oil from Citrus reticulata Blanco Peel

2018 6th International Conference on Mechanical Engineering, Materials Science and Civil Engineering

材料科学;机械制造;土木建筑工程

Hien Tran, Thien^1^2 ; Phat Dao, Tan^1^2 ; Chinh Nguyen, Duy^1 ; Duc Lam, Tri^1 ; Trung Do, Sy^3 ; Quoc Toan, Tran^4 ; Thanh Huong, Nguyen Thi^5 ; Vo, Dai-Viet N.^6 ; Giang Bach, Long^1^2 ; Duy Nguyen, Trinh^1

NTT Hi-Tech Institute, Nguyen Tat Thanh University, Ho Chi Minh City, Viet Nam^1

Faculty of Chemical Engineering and Food Technology, Nguyen Tat Thanh University, Ho Chi Minh City, Viet Nam^2

Institute of Chemistry, Vietnam Academy of Science and Technology, Ha Noi, Viet Nam^3

Institute of Natural Products Chemistry, Vietnam Academy of Science and Technology, Ha Noi, Viet Nam^4

Institute for Tropical Technology, Vietnam Academy of Science and Technology, Ha Noi, Viet Nam^5

Faculty of Chemical and Natural Resources Engineering, Universiti Malaysia Pahang, Malaysia^6

关键词: Box-Behnken design;    Citrus reticulata Blanco;    Confirmation test;    Microwave assisted;    Microwave power;    Optimal conditions;    Quadratic modeling;    Response surface methodology;   

Others  :  https://iopscience.iop.org/article/10.1088/1757-899X/542/1/012043/pdf
DOI  :  10.1088/1757-899X/542/1/012043

来源: IOP

【 摘 要 】

In this research, microwave-assisted hydro-distillation and Response Surface Methodology were selected for optimizing factors affecting the yield of essential oil from Citrus reticulate Blanco peels. This combined process was successfully modeled and optimized using a Box-Behnken design with response surface methodology (RSM). The effects of the material and water ratios, extraction time and microwave power on the extraction essential oils, efficiency of Citrus reticulata Blanco Peel were investigated. The optimal conditions for the Citrus reticulate Blanco peels oils yield were found to be a material and water ratios were 3.1:1mL/g, extraction time was 91.24 min, microwave power at 478 (W). Furthermore, analysis of variance indicated that the proposed quadratic model successfully interpreted the experimental data with coefficients of determination of the predicted R2 of 0.9909 concurred with the adjusted R2 of 0.9826. A confirmation test of the optimal conditions verified the validity of the model, yielding an essential oil efficiency of 5.5