Adjustment of induction high-temperature synthesis to in situ synchrotron study of SHS-mixtures on the example of Ti-Al system

1st International Scientific Practical Conference "Breakthrough Technologies and Communications in Industry"

工业技术（总论）;无线电电子学

Sobachkin, A.V.^1 ; Yu Myasnikov, A.^1 ; Sitnikov, A.A.^1 ; Sharafutdinov, M.R.^2

Polzunov Altai State Technical University, Lenina ave. 46, Barnaul

656038, Russia^1

Budker Institute of Nuclear Physics of Siberian Branch, Russian Academy of Sciences, Acad. Lavrentieva Pr. 11, Novosibirsk

630090, Russia^2

关键词: Diffractometry;    High-temperature synthesis;    In-situ synchrotrons;    Inductive heating;    Kinetics of phase transformation;    Phase formations;    Powder mixtures;    Solid phase reaction;   

Others  :  https://iopscience.iop.org/article/10.1088/1757-899X/483/1/012061/pdf
DOI  :  10.1088/1757-899X/483/1/012061

学科分类：工业工程学

来源: IOP

【 摘 要 】

The paper discusses experimental complex, which allowing to carry out high-temperature synthesis of mechanically activated powder reagents by a method of induction heating in vacuum and inert environment. On the basis of this complex conducted in situ synchrotron research of the specific features of phase formation dynamics in mechanically activated 3Ti + Al powder composition. High temperature synthesis carried out under conditions of high volume inflammation by means of inductive heating. The developed complex is adapted to the method of dynamic diffractometry in synchrotron radiation beams to register the kinetics of phase transformations in the solid-phase reaction of the components of the powder mixture.